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Experimenting with Polymer Capacitors
Blog Deep Dive into ESR, Introduction
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Engagement
  • Author Author: fmilburn
  • Date Created: 8 May 2019 5:06 AM Date Created
  • Views 5124 views
  • Likes 12 likes
  • Comments 31 comments
  • polymer capacitor
  • tenma 72-1020
  • capacitance measurement
  • esr measurement*
  • esr
  • peak esr70
  • ad9850
  • capacitance
  • msp-exp430fr6989
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Deep Dive into ESR, Introduction

fmilburn
fmilburn
8 May 2019

The element14 Experimenting with Polymer Capacitors Challenge is an opportunity to “experiment, test, breadboard, or just play around with Polymer Capacitors” and then show what was learned.  I am grateful to be one of the competitors selected to receive a Polymer Capacitor Kit for my proposal “Deep Dive into ESR”.  Polymer capacitors offer low Equivalent Series Resistance (ESR) and high capacitance in small packages.  Experiments have been carried out which measure ESR and capacitance over a range of values.  A method for measuring ESR using an oscilloscope is presented in addition to use of the Peak ESR70 meter provided in the kit.  Finally, a Panasonic polymer capacitor from the element14 kit is used to reduce ripple from a buck converter.

image

 

In this first post the experiment will be described and the theory behind it explained.  In the next two posts the actual experiments, results and findings will be presented.

 

Introduction

 

Equivalent Series Resistance (ESR) and the actual capacitance of capacitors are among the most important parameters for capacitor performance in a circuit.  While an ideal capacitor has no series resistance, ESR exists in all real world capacitors, albeit with very small values in some of the polymer capacitors investigated here.  There are other deviations from ideal behavior such as series inductance, parallel resistance, and memory effects (dielectric absorbtion) which we will not be addressing.

 

Capacitor ESR not only influences circuit behavior when new, but can worsen over time due to age (e.g. drying out of electrolyte in some capacitors), abuse, and overheating. This increases power dissipation which can start a vicious circle of continued performance reduction.  Thus, the ability to measure both capacitance and ESR quickly with an instrument like the Peak ESR70 is of value.  There is an element14 Cool Tools review of the ESR70 by Michael Wylie here.

 

An oscilloscope can also be used to measure ESR and provides a visual means of assessing the capacitor.  The Peak ESR70 will be used to assess how well the oscilloscope method works.

 

While the Peak ESR70 can be used with the circuit intact in some cases, there are limitations and it isn’t always appropriate.  The experiments performed here will be done on new capacitors outside of a circuit.  ESR is typically quoted by manufacturers at around 100 kHz which is where the Peak ESR70 operates, and also what will be used in the oscilloscope method. The reason for this will be explained shortly.

 

The element14 Kit

 

The Panasonic polymer capacitors in the element14 kit came nicely packaged in their own compartmentalized box.  They are all surface mount.  It is nice to have the assortment as it gives a good idea of the size and range of what is available.

 

My first impression of the Atlas Peak ESR70 is good.  It seems well made and is easy to use.

image

 

Objectives

 

The experiment seeks to understand ESR and how it differs among different polymer capacitors and from aluminum electrolytic and ceramic capacitors.  Application of polymer capacitors will be explored.  To do this we will:

 

  • Describe ESR and how it can be measured
  • Obtain experimental ESR value for various capacitor types and values
  • Obtain experimental capacitance values for various capacitor types and values
  • Compare and summarize findings
  • Evaluate application of polymer capacitors to reduce switching ripple in a DC-DC buck converter

 

Capacitance and ESR will each be measured with two different instruments / methods.  The DC-DC buck converter will be a TI SWIFTTm Power Module.

 

Equipment and Materials

image

 

Equipment

  • Peak ESR70 ESR meter
  • Tenma 72-1020 40,000 count bench multimeter
  • 100 MHz oscilloscope
  • TI MSP430FR6989 Dev BoardAD9850 DDS Synthesizer

 

Materials

  • Panasonic polymer capacitors to be evaluated as listed in the report format section of this post.

 

Similarly rated (capacitance and voltage) aluminum electrolytic and ceramic capacitors readily at hand were also tested.

 

ESR Measurement Theory

 

The method for measuring ESR with an oscilloscope is shown in the following diagram:

image

The square wave generator is modeled as an ideal square wave with a resistor Rout in series.  The capacitor is modeled as an ideal capacitor with a resistor R in series.  Voltage is measured with an oscilloscope.

 

In summary, if the frequency of the square wave is in the 100 kHz range an ideal capacitor begins to approximate a short circuit for the values of capacitance we are interested in.  However, a real capacitor has some equivalent series resistance (ESR) that will cause a voltage drop across the capacitor which can be observed with an oscilloscope.  The method is instructive in that the comparison between ideal and real capacitor behavior can be intuitively grasped from the oscilloscope display.

 

Consider for a moment an ideal capacitor with capacitance, C and being driven by a sinusoidal wave with frequency, f.  Then the reactance is given by the following formula:

 

     Xc = 1 / fC

 

For a 10 uF capacitor or greater capacitor at a frequency of 100 kHz the reactance will be 1 ohm or less which we will assume can be ignored (an assumption to be tested). The voltage drop observed across the capacitor then is due to non-ideal ESR.  Note that we may also see RC time behavior and anomalies due to inductance and transmission line effects.  We will watch for these but disregard them in the calculations.

 

The square wave generator will be modeled as an ideal voltage source with an output resistor. It is necessary to have a known output resistance in order to set up a resistor voltage divider so that the ESR value can be determined.  The square wave will be generated by an AD9850 with an added resistor to make the divider.  There is a description of the AD9850 module and the microcontroller being used here.  Normally a function generator with known output resistance is used and if the proposed method fails a function generator will be obtained.

 

The ESR can be calculated with the resistor voltage divider equation:

 

     Vr = Vfg (R / (R + Rout))

 

Where  Vr      =  Measured voltage across capacitor due to ESR (measured)

            Vfg     = Function generator voltage (measured)

            R        = ESR

            Rout   = output resistance on function generator (known)

        

Rearranging, and solving for ESR we get the equation shown in the diagram.

 

        Vr (R + Rout) = R (Vfg)

Vr (R) + Vr (Rout)  = R (Vfg)

              Vr  (Rout) = R (Vfg – Vr)

                            R = Vr (Rout) / (Vfg – Vr)       formula (1)

 

Experimental Procedure

 

The Peak ESR70 will be used to confirm the results from the oscilloscope / function generator experiments.  It will also be used to confirm capacitance measurements from a good quality bench multimeter.  Tests will be run at room temperature, approximately 20 degrees C.  ESR-70 capacitance probes will be calibrated before starting.  The function generator square wave (100 kHz, ~3V3) and resistor divider settings will be set before starting.  The following procedure will then be followed for each capacitor:

 

Measure capacitance and ESR with ESR70
  1. Measure and record ESR
  2. Measure and record capacitance

 

Measure capacitance use of Tenma 72-102072-1020
  1. Measure and record capacitance

 

Measure voltages with Rigol DS1054Z and Ultrascope
  1. Measure and record open circuit voltage Vfg on oscilloscope
  2. Put the capacitor being tested in place as shown in the diagram
  3. Measure and record voltage across capacitor (ESR)
  4. Look for exponential rise / fall due to RC charge / discharge as shown in diagram and other anomalies.  Record with screenshot.

 

   NOTE:  A Siglent SDS 1102CML 100 MHz oscilloscope was ultimately used in the actual experiments

 

Calculate ESR with formula (1)

 

Discussion of Error

 

None of the instruments being used have calibration certificates and all, with the exception of the ESR70, have been in use for more than a year.  Some pertinent specifications from the instrument manufacturers are given below.

image

 

Testing methods and termination used for ESR measurement with the oscilloscope could introduce error.  The ESR model used is relatively simple and inductance / parallel resistance is not accounted for.  Accordingly, accuracy and resolution for the oscilloscope method has not been determined.

 

Report Format

 

Screenshots and video will be made as appropriate for the experiment.  Results will be recorded in a spreadsheet style tabe with data similar to that listed below for each capacitor evaluated.

imageimage

 

Results will then be plotted and summarized as appropriate in written form along conclusions drawn.

 

A Peek Ahead

 

Shown below, the Peak ESR70 measuring a 4.7 uF aluminum electrolytic....

image

The same 4.7 uF aluminum electrolytic being driven with a 100 kHz square wave is now viewed on the oscilloscope.  The lower blue trace is the square wave and the upper yellow trace shows the voltage drop across the capacitor (ESR) as indicated by the two white lines drawn in and labelled. 

image

The methodology is still being worked but the calculated ESR is roughly 7 ohms with the oscilloscope method and 5.4 ohms with the Peak ESR70.  It probably will  not be possible to measure very low ESR with the oscilloscope.

 

Thanks for the interest - your comments, suggestions and corrections are always appreciated.

Links

  • Deep Dive into ESR, Testing
  • Deep Dive into ESR,  Application
  • AD9850 Frequency Generator Booster Pack
  • Sign in to reply

Top Comments

  • michaelkellett
    michaelkellett over 6 years ago +6
    One of the caps in your kit is 220uF with a claimed ESR of 0.009 ohms (I didn't check them all). At 100 kHz the impedance of an ideal 220uF cap is 0.007 ohms, which is significant. Since one of the benefits…
  • jc2048
    jc2048 over 6 years ago in reply to fmilburn +5
    How many capacitors do you have? If you've got ten of the same type and value, perhaps you could try soldering them in series, measure the ESR with the meter, and then divide the reading by ten to get…
  • michaelkellett
    michaelkellett over 6 years ago in reply to michaelkellett +5
    Here's another paper, showing a better way but using some much more pricey gear (about $5000 for the main box). https://www.omicron-lab.com/fileadmin/assets/Bode_100/ApplicationNotes/Capacitor_ESR_Measurement…
Parents
  • fmilburn
    fmilburn over 6 years ago

    Taking into account Michael's comments about the need for higher frequency and higher current I was thinking about the following modifications to the test circuit:

    image

    Channel 2 should see about 5 millivolts if ESR is 0.01 ohms?  Separately could measure static drain to source on-resistance if that is of use.

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  • fmilburn
    fmilburn over 6 years ago

    Taking into account Michael's comments about the need for higher frequency and higher current I was thinking about the following modifications to the test circuit:

    image

    Channel 2 should see about 5 millivolts if ESR is 0.01 ohms?  Separately could measure static drain to source on-resistance if that is of use.

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  • jc2048
    jc2048 over 6 years ago in reply to fmilburn

    You'd have to be very quick with the scope controls - it's not going to take the capacitor too long to charge to 5V. To stop the capacitor walking off to the rail you need to discharge it too.

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  • michaelkellett
    michaelkellett over 6 years ago in reply to fmilburn

    To measure accurately you need to be a long way from self resonance of the capacitor. You would almost certainly do better with sine wave rather than pulse excitation (because you can estimate the angle between current and voltage).

    You do need a linear power amp that can put out a decent current.

    There are audio amps around that will work at 100kHz (or you could make one).

    A good function generator might manage 200mA peak current which is possibly enough.

     

    MK

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  • fmilburn
    fmilburn over 6 years ago in reply to michaelkellett

    Thanks for the suggestions, I am going to experiment with what I have available.  If I cannot get good measurement on low ESR capacitors I will at least see how low I can go on the others.

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  • michaelkellett
    michaelkellett over 6 years ago in reply to fmilburn

    I though I'd have a go an see how well I could do with lab gear and croc leads.

     

    Here's the setup:

     

    image

     

    Sig gen set for 5V DC and 5V pk-pk, both scope channels AC coupled.

     

    image

     

    This is at 100kHz but I tried 50kHz as well:

     

    image

     

    Not too thrilled by the big difference at the two frequencies - it might even be true but I need more measurements and I'd like

    to calibrate with some better parts.

     

    There are several assumptions, one of the most dodgy is that the two scope channels are perfectly matched for phase despite the different settings.

     

    If I get time I might play some more.

     

    MK

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  • shabaz
    shabaz over 6 years ago in reply to michaelkellett

    Hi Michael!

     

    That's great that the amount of current is feasible for a sig-gen. I'm wondering if the output from your setup could be used directly into this Maxim chip, MAX4211 (PDF doc).

    Basically, if the output was connected to a RC filter, so that the average was available, and then connected to a multi-meter.

    Otherwise, there are analog-multiplier chips from AD, but they are pricey, whereas this Maxim chip is £1.74 in TSSOP package.

    https://uk.farnell.com/maxim-integrated-products/max4211eeue/power-current-sense-2-comp-16tssop/dp/2519303?st=max4211

     

    I just ordered some parts from Farnell, I wish I'd added a few of these to the order : (

    I don't know if it would be accurate, I couldn't see a phase accuracy listed, maybe it is expressed in a different way. Still, it looks like an interesting chip. It's got good bandwidth too (220kHz).

     

    Maybe the cheap DDS modules from e-bay could also be used as a signal source too, although then that needs amplification+buffering (it's about 1Vp-p I think, from memory, at 1.65V (3.3V mid-rail) for the cheap modules.

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